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Volume 30, Issue 18
Reductive Methylation of Secondary Amine ....

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Synthetic Communications

An International Journal for Rapid Communication of Synthetic Organic Chemistry

Volume 30, 2000 - Issue 18

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Original Articles

Reductive Methylation of Secondary Amines Containing Reducible, Hydrolyzable and Sterically Hindered Groups

Bruce A. Davis Neuropsychiatry Research Unit, A114 Medical Research Building, University of Saskatchewan, 103 Wiggins Road, Saskatoon, Saskatchewan, Canada, S7N 5E4

David A. Durden Neuropsychiatry Research Unit, A114 Medical Research Building, University of Saskatchewan, 103 Wiggins Road, Saskatoon, Saskatchewan, Canada, S7N 5E4

Pages 3353-3362 | Received 27 Nov 1999, Published online: 04 Dec 2007

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https://doi.org/10.1080/00397910008086975

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Abstract

Aliphatic secondary amines, including those that are sterically hindered, undergo reductive methylation under mild conditions in high yield using formaldehyde and sodium phosphite solution without reducing or hydrolyzing ethynyl, ester or cyano groups.

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