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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 30, 2000 - Issue 22
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Original Articles

Synthesis of 1,3,6,8-Tetrabromophenanthrene via a Stoichiometric Ullmann Reaction

John M. Farrar Organic Materials Research Group Department of Chemistry, Vanderbilt University, Nashville, TN, 37235
,
Monika Sienkowska Organic Materials Research Group Department of Chemistry, Vanderbilt University, Nashville, TN, 37235
&
Piotr Kaszynski Organic Materials Research Group Department of Chemistry, Vanderbilt University, Nashville, TN, 37235
Pages 4039-4045 | Received 30 Jan 2000, Published online: 04 Dec 2007
 
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Abstract

1,3,6,8-Tetrabromophenantherene (1) is prepared in four steps from 2,4,6-tribromobenzoic acid (4) in an overall yield of 12%. The key transformation used in the synthesis is a stoichiomteric Ullmann reaction.

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