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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 30, 2000 - Issue 10
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Original Articles

A Convenient Method for Selective Mono or Dinitration of Phenol under Mild Conditions

Mohammad Ali Zolfigol Department of Chemistry, College of Science, University of Bu-Ali Sina, zip code 65174, Hamadan, I.R., Iran
,
Ezat Ghaemi Department of Chemistry, College of Science, University of Bu-Ali Sina, zip code 65174, Hamadan, I.R., Iran
&
Elahe Madrakian Department of Chemistry, College of Science, University of Bu-Ali Sina, zip code 65174, Hamadan, I.R., Iran
Pages 1689-1694 | Accepted 01 Aug 1999, Published online: 04 Dec 2007
 
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Abstract

Nitrophenol can be obtained via nitrosation-oxidation of phenol with C2H2O4.2H2O, NaNO2, and wet SiO2 at room temperature in high yield. Direct mono or dinitration of phenol was also performed with C2H2O4. 2H2O, metal nitrates (ionic) and wet SiO2 under different reaction conditions.

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