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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 30, 2000 - Issue 11
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Original Articles

Water Accelerated Sm/TMSCl Reductive System: Debromination of VIC—Dibromides and Reduction of Sodium Alkyl Thiosulfates

Xiaoliang Xu Department of Chemistry, Zhejiang University (Xixi Campus), Hangzhou, 310028, P. R. China
,
Ping Lu Department of Chemistry, Zhejiang University (Xixi Campus), Hangzhou, 310028, P. R. China
&
Yongmin Zhang Department of Chemistry, Zhejiang University (Xixi Campus), Hangzhou, 310028, P. R. China
Pages 1917-1925 | Received 21 May 1999, Published online: 04 Dec 2007
 
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Abstract

A simple and efficient method for the debromination of vic-dibromides to (E)-alkenes and reduction of sodium alkyl thiosulfates to disulfides promoted by Sm/TMSCl/H2O (trace) has been described.

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