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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 30, 2000 - Issue 12
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Original Articles

Microwave Heating in Organic Synthesis: Decarboxylation of Malonic Acid Derivatives in Water

Cynthia Lynn Zara Department of Chemistry, Skidmore College, Saratoga Springs, NY, 12866–1632, USA
,
Thomas Jin Department of Chemistry, Skidmore College, Saratoga Springs, NY, 12866–1632, USA
&
Raymond J. Giguere Department of Chemistry, Skidmore College, Saratoga Springs, NY, 12866–1632, USA
Pages 2099-2104 | Received 10 Jun 1999, Published online: 04 Dec 2007
 
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Abstract

Microwave heating permits rapid decarboxylation (15 min, 80–98% isolated yields) of malonic acids in water when employing a microwave autoclave mode and high reaction temperature and power (190°C; 800 Watts).

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