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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 30, 2000 - Issue 14
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Original Articles

Practical Preparation of 3-Chloro-4-Methoxybenzylamine Hydrochloride

Masaki Endo Process Research, Pharmaceutical Research Institute Bristol-Myers Squibb Candiac, Quebec, Canada, J5R 3W3
&
Jim Douglas Process Research, Pharmaceutical Research Institute Bristol-Myers Squibb Candiac, Quebec, Canada, J5R 3W3
Pages 2609-2612 | Received 19 Oct 1999, Published online: 04 Dec 2007
 
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Abstract

The title compound was prepared in a practical manner by chlorinating 4-methoxybenzylamine with sulfuryl chloride in acetic acid in 79–82% yields with little side reaction.

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