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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 37, 2007 - Issue 5
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Original Articles

Facile Synthesis of 7‐Methoxy‐2‐aryl‐3‐phenyl/or‐H‐8‐[2‐(4,6‐dimethyl‐3,5‐dicarbethoxy‐pyridyl)]‐4H‐1‐benzopyran‐4‐ones

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Pages 795-804 | Received 21 Jul 2006, Published online: 09 Mar 2007
 

Abstract

Condensation of 8‐formyl‐7‐methoxy‐2‐phenyl‐4H‐1‐benzopyran‐4‐ones (5af) with ethyl‐3‐aminocrotonate (6) in glacial acetic acid under Hantzsch conditions afforded 7‐methoxy‐2‐aryl‐3‐phenyl/or‐H‐8‐[2‐(4,6‐dimethyl‐3,5‐dicarbethoxy‐pyridyl)]‐4H‐1‐benzopyran‐4‐ones (7af) in good yields.

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