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An efficient, safe, and viable process has been developed for large-scale preparation of salidroside, a natural product. The process consists of two chemical steps, which produce the salidroside on a multikilogram scale with 72% overall yield and >98% purity. A series of novel salidroside analogs were prepared according to the same method.
This work was financially supported by the National Natural Science Foundation of China (Nos. 20972189, 30901883, and 20802091).
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