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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 13, 1983 - Issue 13
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Original Articles

A Convenient Synthesis of Aldehydes from 1,2-Dimethoxyethenyl-Lithium and Trialkylboranes

Junji Koshino Department of Applied Chemistry, Faculty of Engineering, Hokkaido University, Sapporo, 060, Japan
,
Takahiro Sugawara Department of Applied Chemistry, Faculty of Engineering, Hokkaido University, Sapporo, 060, Japan
,
Toshinobu Yogo Department of Applied Chemistry, Faculty of Engineering, Hokkaido University, Sapporo, 060, Japan
&
Akira Suzuki Department of Applied Chemistry, Faculty of Engineering, Hokkaido University, Sapporo, 060, Japan
Pages 1149-1152 | Published online: 03 Jan 2007
 
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Abstract

The reaction of ate-complexes formed from 1,2-dimethoxy-ethenyllithium and trialkylboranes, with BF3:Et2O followed by hydrolysis with hydrochloric acid gives the corresponding aldehydes in good yields.

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