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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 13, 1983 - Issue 12
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Original Articles

An Efficient Deprotective Method for Allylic Alcohols Protected as Methoxyethoxymethyl (MEM) And Methoxymethyl (MOM) Ethers

H. Monti Laboratoire Associé au C.N.R.S. n° 109, Université d'Aix-Marseille III, Rue Henri Poincaré, 13397, Marseille Cedex 13, France
,
G. Léandri Laboratoire Associé au C.N.R.S. n° 109, Université d'Aix-Marseille III, Rue Henri Poincaré, 13397, Marseille Cedex 13, France
,
M. Klos-ringuet Laboratoire Associé au C.N.R.S. n° 109, Université d'Aix-Marseille III, Rue Henri Poincaré, 13397, Marseille Cedex 13, France
&
C. Corriol Laboratoire Associé au C.N.R.S. n° 109, Université d'Aix-Marseille III, Rue Henri Poincaré, 13397, Marseille Cedex 13, France
Pages 1021-1026 | Published online: 06 Feb 2007
 
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Abstract

Methoxyethoxymethyl ethers (MEM) and methoxymethyl ethers (MOM) of allylic alcohols are readily cleaved by pyridinium paratoluenesulfonate (PPTS) in 2-butanone or t-butyl alcohol. This procedure is also efficient for deprotection of benzylic and aliphatic alcohols.

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