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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 16, 1986 - Issue 2
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Original Articles

Oxidation of Methylquinolines with Nickel Peroxide

David W. Ladner American Cyanamid Company Agricultural Research Division, P.O. Box 400, Princeton, New Jersey, 08560
Pages 157-162 | Published online: 05 Dec 2006
 
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Abstract

Room temperature oxidation of 2-(or 3-)methylquinoline-3-(or 2-)carboxylic acid with 3.25 eq nickel peroxide in aqueous base gives quinoline-2,3-dicarboxylic acid in high yield. No reaction occurs for methylpyridinecarboxylic acids under these conditions.

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