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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 16, 1986 - Issue 3
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Original Articles

The Facile Deselenation of Acetylenic Selenides

João V. Comasseto Instituto de Quīmica da Universidade de SãTo Paulo, Caixa Postal 20780, São Paulo, Brasil
,
Claudio C. Silveira Instituto de Quīmica da Universidade de SãTo Paulo, Caixa Postal 20780, São Paulo, Brasil
,
José T.B. Ferreira Departamento de Quīmica da Universidade, Federal de São Carlos, Caixa Postal 676, São Carlos, S.P., Brasil
&
Valdomiro Catani Departamento de Quīmica da Universidade, Federal de São Carlos, Caixa Postal 676, São Carlos, S.P., Brasil
Pages 283-290 | Published online: 19 Dec 2006
 
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Abstract

Acetylenic selenides react rapidly with m-chloroperbenzoic acid in a mixture of tetra hydrofuran-water. Treatment of the reaction mixture with IN sodium hydroxide leads to the corresponding terminal acetylenes in high yield.

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