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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 16, 1986 - Issue 5
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Original Articles

Chemoselective Oxidation of Secondary Hydroxy Functions Catalyzed by [PMo12O40]3-[C5H5N+(CH2)15 CH3]3

K. Yamawaki Department of applied Chemistry, Kansai University, Senriyama, Suita, Osaka, 564, Japan
,
T. Yoshida Department of applied Chemistry, Kansai University, Senriyama, Suita, Osaka, 564, Japan
,
H. Nishihara Department of applied Chemistry, Kansai University, Senriyama, Suita, Osaka, 564, Japan
,
Y. Ishii Department of applied Chemistry, Kansai University, Senriyama, Suita, Osaka, 564, Japan
&
M. Ogawa Department of applied Chemistry, Kansai University, Senriyama, Suita, Osaka, 564, Japan
Pages 537-541 | Published online: 19 Dec 2006
 
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Abstract

The epoxidation of allylic alcohols with H2O2 catalyzed by a new Mo-species, [PMo12O40]3−[C5H5N+(CH2)15CH3]3 (MPCP), prepared from 12-molybdatophosphoric acid (H3PMo12O40) and cetylpyridinium chloride [C5H5N+(CH2)15CH3 · Cl−], has recently rep0rted.) The high regioselectivity for the epoxidation by this MPCP-H2O2 system was comparable to that of Sharpless method using t-BuOOH as oxidant.

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