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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 17, 1987 - Issue 5
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Original Articles

An Improved, Simple Synthesis of 3-Methyl-2-(4-Methylphenyl) Cyclopenten-2-One: An Important Intermediate in Cuparene Synthesis

Roberto Ballini Dipartimento di Scienze Chimiche Via S. Agostino, 1 62032, Camerino, Italy
,
Marino Petrini Dipartimento di Scienze Chimiche Via S. Agostino, 1 62032, Camerino, Italy
&
Emanuela Marotta Istituto di Chimica Organica dell'università Viale Risorgimento, 4-40136, Bologna, Italy
Pages 543-548 | Published online: 05 Dec 2006
 
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Abstract

Conjugate addition of phenyl-1-methyl-4-(2-nitroethyl) to methyl vinyl ketone in presence of basic a lumina, following by Nef reaction and basic cyclization, affords 3-methyl-2-(4-methyl phenyl) cyclopenten-2-one in good yield.

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