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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 17, 1987 - Issue 13
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Original Articles

Preparation of Diphenylvinylphosphine Oxides by the PCP Process. Choice of the Leaving Group

Philippe Savignac Laboratoire de Chimie du Phosphore et des Métaux de Transition, DCPH-Ecole Polytechnique, 91128, Palaiseau Cedex, France
,
Marie-Paule Teulade Laboratoire de Chimie du Phosphore et des Métaux de Transition, DCPH-Ecole Polytechnique, 91128, Palaiseau Cedex, France
,
Elie Elia Aboujaoude Laboratoire des Composés Organophosphorés, INSA-IRCOF, BP 08, 76130, Mont-Saint-Aignan, France
&
Noel Collignon Laboratoire des Composés Organophosphorés, INSA-IRCOF, BP 08, 76130, Mont-Saint-Aignan, France
Pages 1559-1568 | Published online: 06 Dec 2006
 
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Abstract

Carbanionic conversion of alkyl into vinylphosphonates is extended to the preparation of diphenylvinylphosphine oxides. Obtention of pure products in optimized yields is closely related to the choice of the phosphate leaving group.

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