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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 17, 1987 - Issue 13
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Original Articles

Polymer-Supported Phosphine-Halogen Complexes 41. Improved Formylation of Alcohols with Dimethylformamide

Romualdo Caputo Dipartimento di Chimica, Organica e Biologica dell Università, Via Mezzocannone, 16, I-80134, Napoli, (Italy)
,
Carla Ferreri Dipartimento di Chimica, Organica e Biologica dell Università, Via Mezzocannone, 16, I-80134, Napoli, (Italy)
&
Giovanni Palumbo Dipartimento di Chimica, Organica e Biologica dell Università, Via Mezzocannone, 16, I-80134, Napoli, (Italy)
Pages 1629-1636 | Published online: 06 Dec 2006
 
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Abstract

A new, very convenient procedure for smooth conversion of primary and secondary alcohols to their corresponding formic acid esters is described. This is based on the use of modified Vilsmeier Haak adducts, obtained from N, N-dimethylformamide and polymersupported triarylphosphine-halogen complexes.

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