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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 17, 1987 - Issue 10
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Original Articles

Reduction of Ni(ACAC)2 Under Carbonylative Conditions: A Suitable Procedure for Small Scale Production of Ni (CO)4

F. Boix Departament Química Orgànica Biològica, C.I.D., C.S.I.C., Jorge Girona Salgado 18-26, 08034, Barcelona, Spain
,
F. Camps Departament Química Orgànica Biològica, C.I.D., C.S.I.C., Jorge Girona Salgado 18-26, 08034, Barcelona, Spain
,
J. Coll Departament Química Orgànica Biològica, C.I.D., C.S.I.C., Jorge Girona Salgado 18-26, 08034, Barcelona, Spain
,
J. M. Moretó Departament Química Orgànica Biològica, C.I.D., C.S.I.C., Jorge Girona Salgado 18-26, 08034, Barcelona, Spain
&
J. Torras Departament Química Orgànica Biològica, C.I.D., C.S.I.C., Jorge Girona Salgado 18-26, 08034, Barcelona, Spain
Pages 1149-1153 | Published online: 05 Dec 2006
 
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Abstract

Reduction of diluted solutions of anhydrous Ni(II) acetylacetonate in THF by reducing alkylating agents such as DIBAH, n-Bu Li or PrMgBr in the presence of carbon monoxide gave practically quantitative yields of Ni (CO)4.

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