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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 17, 1987 - Issue 10
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Original Articles

Allylic Oxidation of Δ5-Steroids with Pyridinium Chlorochromate (PCC) and Pyridinium Dichromate (PDC)

Edward J. Parish Department of Chemistry, Auburn University, AL, 36849
&
Tsao-Yi Wei Department of Chemistry, Auburn University, AL, 36849
Pages 1227-1233 | Published online: 05 Dec 2006
 
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Abstract

Pyridinium chlochromate (PCC), in refluxing benzene, or dimethyl sulfoxide, and pyridinium dichromate (PDC) in pyridine, have been found to be effective reagents for the allylic oxidation of Δ5-steroids to yield the corresponding α, β - unsaturated ketones.

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