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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 17, 1987 - Issue 10
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Original Articles

Resolution of (±)-2,3-Dihydro-2-phenyl-4(1H)-Quinolone

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Pages 1235-1245 | Published online: 05 Dec 2006
 

Abstract

The resolution of (±)-2,3-dihydro-2-phenyl-4(1H)-quinolone into individual enantiomers was achieved using the optically active oxo reagent (-)-5-(α-phenethyl)-semioxamazide. The enantiomeric purity was checked by 1H-NMR using the chiral lanthanide shift reagent Eu(hfc)3.

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