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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 19, 1989 - Issue 3-4
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Original Articles

An Efficient Procedure for the Synthesis of p-Anisidine Phenylglyoxal Imine from Acetophenone

R. Desmond Merck Sharp and Dohme Research Laboratories Division of Merck and Co., Inc., Rahway, New Jersey, 07065
,
S. Mills Merck Sharp and Dohme Research Laboratories Division of Merck and Co., Inc., Rahway, New Jersey, 07065
,
R. P. Volante Merck Sharp and Dohme Research Laboratories Division of Merck and Co., Inc., Rahway, New Jersey, 07065
&
I. Shinkai Merck Sharp and Dohme Research Laboratories Division of Merck and Co., Inc., Rahway, New Jersey, 07065
Pages 379-385 | Received 07 Jun 1988, Published online: 23 Oct 2006
 
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Abstract

An efficient procedure for the oxidation of acetophenone to phenylglyoxal and its subsequent in situ conversion to the title compound is described herein.

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