Photochemical Synthesis of Aporphines: (±)-Glaucine, (±)-Norglaucine and (±)-Dehydronorglaucine

Sandeep Gupta Medicinal Chemistry Division, Central Drug Research Institute, Lucknow, 226001, INDIA; Boyce Thompson Institute, Cornell University, Ithaca, NY, 14853, USA

Dewan S. Bhakuni Medicinal Chemistry Division, Central Drug Research Institute, Lucknow, 226001, INDIA

Abstract

Photochemical cyclization of 3 afforded 5, 4 and 8.5 on LAH reduction furnished (±)-glaucine (6) and on treatment with ethanolic HCl afforded (±)-norglaucine (7). 10 obtained by the photocyclization of 9 was converted into 7 and 11 via 12.

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Photochemical Synthesis of Aporphines: (±)-Glaucine, (±)-Norglaucine and (±)-Dehydronorglaucine

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Photochemical Synthesis of Aporphines: (±)-Glaucine, (±)-Norglaucine and (±)-Dehydronorglaucine

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