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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 19, 1989 - Issue 5-6
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Original Articles

New Preparation of α,β-Unsaturated Esters from 1-Alkenes Via Two Carbon Homologation Route. Synthesis of Queen Substance

Hiroyuki Ishibashi Kyoto Pharmaceutical University, Misasagi, Yamashina, Kyoto, 607, Japan
,
Minako Ohnishi Kyoto Pharmaceutical University, Misasagi, Yamashina, Kyoto, 607, Japan
,
Toshihiko Senda Kyoto Pharmaceutical University, Misasagi, Yamashina, Kyoto, 607, Japan
&
Masazumi Ikeda Kyoto Pharmaceutical University, Misasagi, Yamashina, Kyoto, 607, Japan
Pages 857-864 | Received 28 Apr 1988, Published online: 24 Oct 2006
 
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Abstract

2-Methylthio-4-alkenoic esters prepared from 1-alkenes and ethyl methylsulfinylacetate are converted into α,β-unsaturated esters via hydrogenation, oxidation, and thermolysis. This method was applied to the synthesis of queen substance.

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