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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 19, 1989 - Issue 9-10
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Original Articles

N-Formylglycine t-Butyl Ester

, &
Pages 1487-1491 | Received 08 Dec 1988, Published online: 24 Oct 2006
 

Abstract

An improved synthesis of the title compound is described. N,N-Diformylglycine t-butyl ester 3, which was previously unknown, was isolated as a by-product from the preparation of 1. Additionally, another method for the preparation of 1 is described which consists of the reaction of sodium diformylamide 5 with the chloroester 4 in DMF.

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