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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 19, 1989 - Issue 9-10
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Original Articles

A General Preparation of 2-Acyl-3-(Phenylthio)-1, 3-Butadienes

Shang-Shing P. Chou Department of Chemistry, Fu Jen University Taipei, Taiwan, 24205, Republic of China
,
Der-Jen Sun Department of Chemistry, Fu Jen University Taipei, Taiwan, 24205, Republic of China
&
Shiow-Jyi Weh Department of Chemistry, Fu Jen University Taipei, Taiwan, 24205, Republic of China
Pages 1593-1602 | Received 12 Jul 1988, Published online: 24 Oct 2006
 
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Abstract

The title dienes 1 are prepared by thermolysis of 3-sulfolenes 2, which are readily obtained by ultrasound promoted allylzincation of bromides 4 with aldehydes followed by PCC oxidation.

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