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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 19, 1989 - Issue 11-12
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Original Articles

An Alternative Method for the Stereospecific Synthesis of Conjugated Alkenynes Via the Copper (I) Iodide Assisted Cross-Coupling Reaction of 1-Akyens with Haloalkenes

Takuji Ogawa Department of Chemistry, Faculty of Science, Ehime University, Bunkyo-cho, Matsuyama, 790, Japan
,
Kumiko Kusume Department of Chemistry, Faculty of Science, Ehime University, Bunkyo-cho, Matsuyama, 790, Japan
,
Miyuki Tanaka Department of Chemistry, Faculty of Science, Ehime University, Bunkyo-cho, Matsuyama, 790, Japan
,
Kazuo Hayami Department of Chemistry, Faculty of Science, Ehime University, Bunkyo-cho, Matsuyama, 790, Japan
&
Hitomi Suzuki Department of Chemistry, Faculty of Science, Ehime University, Bunkyo-cho, Matsuyama, 790, Japan
Pages 2199-2207 | Received 05 Dec 1988, Published online: 24 Oct 2006
 
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Abstract

Conjugated alkenynes were prepared stereospecifically in moderate to good yields by heating haloalkenes with 1-alkynes in the presence of copper(I) iodide in hexamethylphosphoric triamide (HMPA).

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