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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 19, 1989 - Issue 15
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Original Articles

A Synthesis of Fused Butenoudes

Gerald L. Larson Department of Chemistry, University of Puerto Rico, Rio Piedras, PR 00931 and Hüls America, Inc./Petrarch Systems, Bartram Road, Bristol, PA, 19007; Hüls Americ, Inc./Petrarch Systems
,
J. Antonio Prieto Department of Chemistry, University of Puerto Rico, Rio Piedras, PR 00931 and Hüls America, Inc./Petrarch Systems, Bartram Road, Bristol, PA, 19007; University of Puerto Rico
&
Patricia Gonzalez Department of Chemistry, University of Puerto Rico, Rio Piedras, PR 00931 and Hüls America, Inc./Petrarch Systems, Bartram Road, Bristol, PA, 19007; University of Puerto Rim. NIGMS-MARC Faculty Fellow 1981-1986
Pages 2779-2782 | Received 01 May 1989, Published online: 24 Oct 2006
 
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Abstract

It has been shown that tert-butyldimethylsilylated (Z) 2-carboethoxymethylene cycloalkanols are readily desilylated with concomitant cyclization to give the corresponding butenolides. The (E) isomers are desilylated, but not cyclized under these conditions.

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