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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 20, 1990 - Issue 19
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Original Articles

Synthesis of Dienals by Condensation of Carbonyl Compounds with a New Reagent, the 4-Lithio-1-trimethylsiloxybutadiene

Beatriz Contreras Laboratoire de Chimie Organique, Unité de recherche Associée au CNRS n° 464, Université de Rouen, B.P. 68, 76134, MONT SAINT AIGNAN CEDEX, France
,
Lucette Duhamel Laboratoire de Chimie Organique, Unité de recherche Associée au CNRS n° 464, Université de Rouen, B.P. 68, 76134, MONT SAINT AIGNAN CEDEX, France
&
Gérard Ple Laboratoire de Chimie Organique, Unité de recherche Associée au CNRS n° 464, Université de Rouen, B.P. 68, 76134, MONT SAINT AIGNAN CEDEX, France
Pages 2983-2990 | Received 31 Jul 1990, Published online: 24 Oct 2006
 
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Abstract

Carbonyl compounds 2 are converted into conjugated dienals 3. in a one pot reaction, by a condensation with lithio-4 trimethylsiloxybutadiene, followed by a mild acidic hydrolysis.

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