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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 20, 1990 - Issue 19
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Original Articles

In Situ Reagents For Thionation of Amides, Peptides and Lactams

Denis Brillon Institut Armand-Frappier, Université du Québec, 531 Boul. des Prairies, Laval, P. Québec, CanActa H7N 4Z3
Pages 3085-3095 | Received 20 Aug 1990, Published online: 24 Oct 2006
 
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Abstract

An in situ reagent 1A for thionation of amides, peptides and lactams is prepared from phosphorus decasulfide/sodium carbonate (1:1ratio) in THF at 25°C.

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