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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 20, 1990 - Issue 21
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Original Articles

Preparation of the N-(2-Bromo-2-Nitroethenyl) Benzenamine: The First One-Pot Synthesis of a β-Halo-β-Nitroenamine

Daniel Dauzonne Demerseman Service de Chimie, Institut Curie, URA 1387 P CNRS, 26 rue d'Ulm, 75231, Paris Cedex 05, France
,
Anne Fleurant Demerseman Service de Chimie, Institut Curie, URA 1387 P CNRS, 26 rue d'Ulm, 75231, Paris Cedex 05, France
,
Pierre Demerseman Service de Chimie, Institut Curie, URA 1387 P CNRS, 26 rue d'Ulm, 75231, Paris Cedex 05, France
,
Michel Cotrait Laboratoire de Cristallographie, Université de Bordeaux 1, UA 144 CNRS, 351 Cours de la Libération, 33405, Talence Cedex, France
&
Jean-Pierre Bideau Laboratoire de Cristallographie, Université de Bordeaux 1, UA 144 CNRS, 351 Cours de la Libération, 33405, Talence Cedex, France
Pages 3339-3345 | Received 17 Sep 1990, Published online: 24 Oct 2006
 
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Abstract

Bromonitromethane, triethyl orthoformate and aniline react together, in a one-flask procedure, to afford the title compound.

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