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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 20, 1990 - Issue 2
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Original Articles

Amidrazones 13. A Convenient Method for the Preparation of 1-Alkyl-1-methylhydrazines

Richard F. Smith Department of Chemistry, State University College of Arts and Science, Geneseo, NY, 14454
,
Keith A. Brophy Department of Chemistry, State University College of Arts and Science, Geneseo, NY, 14454
,
George Rodriguez Department of Chemistry, State University College of Arts and Science, Geneseo, NY, 14454
,
Lisa A. Dennis Department of Chemistry, State University College of Arts and Science, Geneseo, NY, 14454
&
William J. Ryan Department of Chemistry, State University College of Arts and Science, Geneseo, NY, 14454
Pages 183-188 | Received 28 Aug 1989, Published online: 24 Oct 2006
 
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Abstract

An efficient one-pot procedure for the preparation of 1-alkyl-1-methylhydrazines from methylhydrazine via base-promoted hydrolysis of 1-alkyl-3-amino-4, 5-dihydro-1-methyl-1H-pyrazolium halides (3) is described.

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