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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 20, 1990 - Issue 3
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Original Articles

An Electrochemical Preparation of Methyl Methanethiolsulfonate

Pedro D. Machion Instituto de Quírnica, Universidade de São Paulo, C.P. 20.780-01.498, São Paulo, S.P. Brazil
,
Vera L. Pardini Instituto de Quírnica, Universidade de São Paulo, C.P. 20.780-01.498, São Paulo, S.P. Brazil
&
Hans Viertler Instituto de Quírnica, Universidade de São Paulo, C.P. 20.780-01.498, São Paulo, S.P. Brazil
Pages 365-370 | Received 20 Sep 1989, Published online: 24 Oct 2006
 
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Abstract

Methyl methanethiolsulfonate is conveniently prepared, in good yields, by electrochemical oxidation of dimethyl disulfide, in aqueous acetonitrile, at constant current.

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