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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 20, 1990 - Issue 3
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Original Articles

Mild and Reversible Friedel-Crafts Acylation: Synthesis of 6-Acyl-2-methoxynaphthalenes

Claudio Giordano Istituto di Ricerca Chimica “G. Zambon” Zambon Group S.p.A., Via Cimabue, 26/28 20032 Cormano, Milan, Italy
,
Marco Villa Istituto di Ricerca Chimica “G. Zambon” Zambon Group S.p.A., Via Cimabue, 26/28 20032 Cormano, Milan, Italy
&
Rita Annunziata Dipartimento di Chimica Organica ed Industriale, Università degli Studi di Milano, Viale Golgi, 19, Milan, Italy
Pages 383-392 | Received 25 Sep 1989, Published online: 24 Oct 2006
 
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Abstract

A new practical method for large scale preparation of 2-acyl-6-methoxynaphthalenes 3 is reported. The selectivity toward 3 is due to reversibility of the Friedel-Crafts acylation and to the thermodynamic stability of 3.

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