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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 20, 1990 - Issue 10
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Original Articles

Facile Conversion of Primary and Secondary Alcohols to Alkyl Iodides

Gordon L. Lange Guelph-Waterloo Centre for Graduate Work in Chemistry Department of Chemistry and Biochemistry, University of Guelph, Guelph, Ontario, N1G 2W1, Canada
&
Christine Gottardo Guelph-Waterloo Centre for Graduate Work in Chemistry Department of Chemistry and Biochemistry, University of Guelph, Guelph, Ontario, N1G 2W1, Canada
Pages 1473-1479 | Received 27 Feb 1990, Published online: 24 Oct 2006
 
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Abstract

A convenient, simple procedure is described for the conversion of a variety of primary and secondary alcohols to iodides in yields ranging from 60–98%. The method employs the Ph3P/imidazole/I2 combination of reagents in the solvent dichloromethane.

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