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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 20, 1990 - Issue 15
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Original Articles

An Efficient Procedure for Tri(2-Methoxyphenyl)Phosphine

L. Brandsma Department of Synthetic Organic Chemistry, Debye Institute, University of Utrecht, Padualaan 8, 3584, CH, Utrecht, The Netherlands
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H. D. Verkruijsse Department of Synthetic Organic Chemistry, Debye Institute, University of Utrecht, Padualaan 8, 3584, CH, Utrecht, The Netherlands
Pages 2273-2274 | Received 16 May 1990, Published online: 24 Oct 2006
 
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Abstract

Tri(2-methoxyphenyl)phosphine has been prepared in an excellent yield by metallating methoxybenzene with n-BuLi. TMEDA in hexane and subsequently reacting the resulting lithiomethoxybenzene with phosphorus trichloride in a mixture of THF and hexane.

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