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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 20, 1990 - Issue 15
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Original Articles

Hypervalent Iodine Oxidation of Amines in the Presence of Nitroso Compounds: A Method for the Preparation of Unsymmetrically Substituted Azoxy Compounds

R. M. Moriarty Department of Chemistry, University of Illinois at Chicago, P.O. Box 4348, Chicago, Illinois, 60607
,
T. E. Hopkins Department of Chemistry, University of Illinois at Chicago, P.O. Box 4348, Chicago, Illinois, 60607
,
I. Prakash Department of Chemistry, University of Illinois at Chicago, P.O. Box 4348, Chicago, Illinois, 60607
,
B. K. Vaid Department of Chemistry, University of Illinois at Chicago, P.O. Box 4348, Chicago, Illinois, 60607
&
R. K. Vaid Department of Chemistry, University of Illinois at Chicago, P.O. Box 4348, Chicago, Illinois, 60607
Pages 2353-2357 | Received 01 Jun 1990, Published online: 24 Oct 2006
 
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Abstract

Various amines and amino derivatives such as (tert-butylamine, 4-amino-1,2,4-triazole-p-toluenesulfonamide), and cyanamide, when treated with |(diacetoxy)iodo|benzene in the presence of nitroso compounds (2) yield unsymmetrically substituted azoxy compounds (3).

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