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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 20, 1990 - Issue 1
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Original Articles

Exclusive Ortho Cyanation and Alkylthiocarbonylation of Anilines and Phenols Using Boron Trichloride

Makoto Adachi Shionogi Research Laboratories, Shionogi & Co., Ltd., Fukushima-ku, Osaka, 553, Japan
&
Tsutomu Sugasawa Shionogi Research Laboratories, Shionogi & Co., Ltd., Fukushima-ku, Osaka, 553, Japan
Pages 71-84 | Received 02 Aug 1989, Published online: 24 Oct 2006
 
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Abstract

Use of boron trichloride with or without an additional Lewis acid makes possible a one-step synthesis of 2-cyano and 2-alkylthiocarbonyl anilines and phenols.

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