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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 20, 1990 - Issue 1
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Original Articles

Synthesis of Perfluoroacrylic Acid from 3-Hydrotetrafluoropropanol

T. Nguyen C.N.R.S.-C.E.R.C.O.A. 2, rue Henri Dunant, 94320, Thiais, (France)
&
C. Wakselman C.N.R.S.-C.E.R.C.O.A. 2, rue Henri Dunant, 94320, Thiais, (France)
Pages 97-99 | Received 04 Aug 1989, Published online: 24 Oct 2006
 
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Abstract

Perfluoroacrylic acid 1a was prepared from tetrafluoropropanol-1 2 by reaction of an alkyl lithium yielding trifluoroacrylic alcohol 3, followed by oxidation of the latter with potassium permanganate, after protection of the double bond.

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