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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 20, 1990 - Issue 1
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Original Articles

Microwave Irradiation Plus Solid-Liquid Phase Transfer Catalysis Without Solvent: Further Improvement in Anionic Activation

Georges Bram Laboratoire des Réactions Sélectives sur Supports, ICKO, UA 478 du CNRS, Université Paris-Sud, Bàtiment 410, 91405, Orsay Cedex, (France)
,
André Loupy Laboratoire des Réactions Sélectives sur Supports, ICKO, UA 478 du CNRS, Université Paris-Sud, Bàtiment 410, 91405, Orsay Cedex, (France)
&
Mustapha Majdoub Laboratoire des Réactions Sélectives sur Supports, ICKO, UA 478 du CNRS, Université Paris-Sud, Bàtiment 410, 91405, Orsay Cedex, (France)
Pages 125-129 | Received 03 Aug 1989, Published online: 24 Oct 2006
 
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Abstract

Owing to cumulative effects of microwave irradiation and solid-liquid PTC without solvent methodology, conditions for alkylations of potassium acetate by n-octyl or n-cetyl halides are nearly quantitative within 2 minutes on appreciable quantities.

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