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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 20, 1990 - Issue 4
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Original Articles

A Convenient Synthesis of Tertiary Isothiocyanates and Acyl Isothiocyanates Using Phosphoryl Isothiocyanate

Ladislav Kniežo Department of Organic Chemistry, P. J. Šafárik University, 041 67, Košice, Czechoslovakia
&
Juraj Bernát Department of Organic Chemistry, P. J. Šafárik University, 041 67, Košice, Czechoslovakia
Pages 509-513 | Received 04 Oct 1989, Published online: 24 Oct 2006
 
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Abstract

Phosphoryl isothiocyanate, PO(NCS)3, reacts readily with tertiary alcohols and carboxylic acids, giving the respective tertiary isothiocyanates and acyl isothiocyanates in good yields and purity.

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