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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 21, 1991 - Issue 4
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Original Articles

Asymmetric Synthesis XXIII.1 A 100% cis Diastereoselectivity in the SYnthesis of Enantiomerically Pure 2,6-Dialkylpiperidines

Emmanuel Theodorakis Institut de Chimie des Substances Naturelles CNRS, 91198, Gif-sur-Yvette, Cedex, France
,
Jacques Royer Institut de Chimie des Substances Naturelles CNRS, 91198, Gif-sur-Yvette, Cedex, France
&
Henri-Philippe Husson Institut de Chimie des Substances Naturelles CNRS, 91198, Gif-sur-Yvette, Cedex, France
Pages 521-529 | Received 13 Dec 1990, Published online: 23 Sep 2006
 
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Abstract

Enantiomerically pure (+)-(2S,6R)-2-propyl-6-methyl-piperidine 6 has been obtained in 4 steps, 66% overall yield and without separation of diastereomers from the chiral 2-cyano-6-oxazolopiperidine synthon 1c derived from (+)-1,2-diphenyl-2-aminoethanol

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