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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 21, 1991 - Issue 8-9
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Original Articles

Synthesis of Vinca Alkaloids and Related Compounds. PART LVIII. A Novel Formal Synthesis of (−)-Criocerine from (+)-Vincamine

István Moldvai Central Research Institute for Chemistry, Hungarian Academy of Sciences, H-1025, Budapest, POB 17, Hungary
,
Csaba Szántay Jr. Chemical Works of Gedeon Richter, NMR Laboratory of the Research, Department of Physical Chemistry, H-1475, Budapest, POB 27, Hungary
&
Csaba Szántay Central Research Institute for Chemistry, Hungarian Academy of Sciences, H-1025, Budapest, POB 17, Hungary
Pages 965-967 | Received 11 Feb 1991, Published online: 23 Sep 2006
 
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Abstract

18-lodo criocerine (3), a synthetic precursor to (−)-criocerine (1), was prepared from (+)-vincamine (4) via a new one-step procedure. Full 1H and 13C NMR assignments for 3 are also given.

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