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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 21, 1991 - Issue 20
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Original Articles

Dihalogenation of β-Keto Sulfides. Synthesis of α-Keto Methyl Esters and α-Keto S-Phenyl Thioesters

Carlos C. Fortes Departamento de Química, Universidade de Brasilia DF, 70910, Brazil
,
Carlos R. O. Souto Departamento de Química, Universidade de Brasilia DF, 70910, Brazil
&
Esmeralda A. Okino Departamento de Química, Universidade de Brasilia DF, 70910, Brazil
Pages 2045-2052 | Received 29 May 1991, Published online: 23 Sep 2006
 
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Abstract

α-Keto esters and α-Keto S-Phenyl Thioesters are synthesized from β-keto sulfides by dihalogenation with sulfuryl chloride followed by solvolysis with methanol and acetone/water respectively.

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