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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 21, 1991 - Issue 2
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Original Articles

TiCl4 induced N-Methyleneamine Equivalents: A New Route to Aminoacetonitriles

Hyun-Joon Ha Division of Chemistry, Korea Institute of Science and Technology, P.O. Box 131 Cheongryang, Seoul, 130-650, Korea
,
Gong-Sil Nam Division of Chemistry, Korea Institute of Science and Technology, P.O. Box 131 Cheongryang, Seoul, 130-650, Korea
&
Kyong Pae Park Division of Chemistry, Korea Institute of Science and Technology, P.O. Box 131 Cheongryang, Seoul, 130-650, Korea
Pages 155-160 | Received 06 Nov 1990, Published online: 23 Sep 2006
 
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Abstract

TiCl4 induced N-methyleneamine equivalents from hexahydro-1,3,5-triazines or N-(methoxymethyl)amines were reacted with trimethylsilyl cyanide to give aminoacetonitriles in 40–90% yield.

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