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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 21, 1991 - Issue 2
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Original Articles

A Convenient High-Yield Procedure for the β-Hydroxyethylation of Acetylenes with Epoxyethane in Liquid Ammonia

H. D. Verkruijsse Department of Preparative Organic Chemistry of, the University, Debye Institute Padualaan, 8, 3584, CH, Utrecht, The Netherlands
&
L. Brandsma Department of Preparative Organic Chemistry of, the University, Debye Institute Padualaan, 8, 3584, CH, Utrecht, The Netherlands
Pages 235-237 | Received 21 Nov 1990, Published online: 23 Sep 2006
 
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Abstract

3-Butyn-1-ol and homologues, RC°CCH2CH2OH (R=H or alkyl), have been obtained in excellent yields from alkynyllithium derivatives, RC°CLi, and epoxyethane in liquid ammonia.

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