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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 21, 1991 - Issue 21
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Original Articles

Synthesis of Vinyl and β-Phthalimido Ketones

Philip D. Hammen Central Research Division, Pfizer Inc., Groton, CT, 06340
,
Andrew C. Braisted Central Research Division, Pfizer Inc., Groton, CT, 06340
&
David L. Northrup Central Research Division, Pfizer Inc., Groton, CT, 06340
Pages 2157-2163 | Received 14 Jun 1991, Published online: 01 Oct 2010
 
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Abstract

Vinyl ketones are prepared by reaction of an aldehyde with a vinyl Grignard reagent followed by a Swern oxidation. β-Phthalimido ketones are then obtained by 1,4-addition of phthalimide.

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