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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 21, 1991 - Issue 21
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Original Articles

Microwave Heating in Synthesis: Preparation of Allyldiphenylphosphine Oxide

Raymond J. Giguere Department of Chemistry and Physics, Skidmore College, Saratoga Springs, New York, 12866-1632
&
Brad Herberich Department of Chemistry and Physics, Skidmore College, Saratoga Springs, New York, 12866-1632
Pages 2197-2201 | Received 17 Jun 1991, Published online: 01 Oct 2010
 
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Abstract

A new one-pot synthesis of allyldiphenyl-phosphine oxide has been developed using a tandem Sn2′ / Michaelis-Arbuzov sequence. The application of microwave heating lowers the reaction time significantly.

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