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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 22, 1992 - Issue 12
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Original Articles

A Convenient One-Pot Preparation of Symmetrical Polymethoxyanthracenes

John J. Fitzgerald Department of Chemistry, The Pennsylvania State University, University Park, Pennsylvania, 16802, USA
,
Neville E. Drysdale Department of Chemistry, The Pennsylvania State University, University Park, Pennsylvania, 16802, USA
&
R. A. Olofson Department of Chemistry, The Pennsylvania State University, University Park, Pennsylvania, 16802, USA
Pages 1807-1812 | Accepted 26 Feb 1992, Published online: 23 Sep 2006
 
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Abstract

Symmetrical polymethoxyanthracenes are rapidly made and easily isolated in moderate yield by treatment of appropriately substituted (methoxy)n halobenzenes with lithium 2,2,6,6-tetramethylpiperidide (LTMP) in refluxing THF.

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