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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 22, 1992 - Issue 13
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Original Articles

Oxidation of Activated Halides to Aldehydes and Ketones by N-Methylmorpholine-N-oxide

William P. Griffith Department of Chemistry, Imperial College of Science, Technology and Medicine, South Kensington, London, SW7 2AY, U.K.
,
Jenny M. Jolliffe Department of Chemistry, Imperial College of Science, Technology and Medicine, South Kensington, London, SW7 2AY, U.K.
,
Steven V. Ley Department of Chemistry, Imperial College of Science, Technology and Medicine, South Kensington, London, SW7 2AY, U.K.
,
Karsten F. Springhorn Department of Chemistry, Imperial College of Science, Technology and Medicine, South Kensington, London, SW7 2AY, U.K.
&
Peter D. Tiffin Department of Chemistry, Imperial College of Science, Technology and Medicine, South Kensington, London, SW7 2AY, U.K.
Pages 1967-1971 | Accepted 06 Mar 1992, Published online: 23 Sep 2006
 
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Abstract

N-methylmorpholine-N-oxide (NMO) in acetonitrile solution will oxidise activated primary halides to aldehydes and secondary halides to ketones in good yields at room temperature.

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