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Synthetic Communications
An International Journal for Rapid Communication of Synthetic Organic Chemistry
Volume 22, 1992 - Issue 19
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Original Articles

A Refined Method for the Removal of the Methoxymethyl (MOM) Protecting Group for Carbinols with Acidic Ion-Exchange Resin

Hideharu Seto Research School of Chemistry, Australian National University, Canberra, ACT 2601, Australia; The Institute of Physical and Chemical Research, Hirosawa, Wako, Saitama, 351-01, Japan
&
Lewis N. Mander Research School of Chemistry, Australian National University, Canberra, ACT 2601, Australia
Pages 2823-2828 | Accepted 23 May 1992, Published online: 23 Sep 2006
 
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Abstract

The methoxymethyl protecting group for carbinols is best removed from acid-sensitive substrates by hydrolysis in aqueous methanol using a cationic exchange resin (Dowex-50W).

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