Selective Oxidation of Steroidal Homoallylic Alcohols Using Pyridinium Chlorochromate (PPC)

Edward J. Parish Department of Chemistry, Auburn University, AL, 36849-5312

Chi Luo Department of Chemistry, Auburn University, AL, 36849-5312

Sarawanee Parish Department of Chemistry, Auburn University, AL, 36849-5312

Robert W. Heidepriem Department of Chemistry, Auburn University, AL, 36849-5312

Abstract

Pyridinium chlorochromate (PCC), in the presence of anhydrous calcium carbonate, has been found to be an effective and convenient reagent for the selective oxidation of steroidal homoallylic alcohols to the corresponding β,δ-unsaturated ketones in good yield.

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Selective Oxidation of Steroidal Homoallylic Alcohols Using Pyridinium Chlorochromate (PPC)

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Selective Oxidation of Steroidal Homoallylic Alcohols Using Pyridinium Chlorochromate (PPC)

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